Bonding of resin cement to zirconia with high pressure primer coating

Chen Wang, Li Na Niu, Ying Jie Wang, Kai Jiao, Yan Liu, Wei Zhou, Li Juan Shen, Ming Fang, Meng Li, Xiang Zhang, Franklin Chi Meng Tay, Ji Hua Chen

Research output: Contribution to journalArticlepeer-review

23 Scopus citations


Objectives: To investigate the effect of air-drying pressure during ceramic primer coating on zirconia/resin bonding and the surface characteristics of the primed zirconia. Methods: Two ceramic primers (Clearfil Ceramic Primer, CCP, Kuraray Medical Inc. and Z-Prime Plus, ZPP, Bisco Inc.) were applied on the surface of air-abraded zirconia (Katana zirconia, Noritake) and dried at 4 different air pressures (0.1-0.4 MPa). The primed zirconia ceramic specimens were bonded with a resin-based luting agent (SA Luting Cement, Kuraray). Microshear bond strengths of the bonded specimens were tested after 3 days of water storage or 5,000 x thermocycling (n = 12). Failure modes of the fractured specimens were examined with scanning electron miscopy. The effects of air pressure on the thickness of the primer layers and the surface roughness (S a) of primed zirconia were evaluated using spectroscopic ellipsometry (n = 6), optical profilometry and environmental scanning electron microscopy (ESEM) (n = 6), respectively. Results: Clearfil Ceramic Primer air-dried at 0.3 and 0.4 MPa, yielding significantly higher μSBS than gentle air-drying subgroups (p<0.05). Compared to vigorous drying conditions, Z-Prime Plus air-dried at 0.2 MPa exhibited significantly higher μSBS (p<0.05). Increasing air-drying pressure reduced the film thickness for both primers. Profilometry measurements and ESEM showed rougher surfaces in the high pressure subgroups of CCP and intermediate pressure subgroup of ZPP. Conclusion: Air-drying pressure influences resin/zirconia bond strength and durability significantly. Higher air-drying pressure (0.3-0.4 MPa) for CCP and intermediate pressure (0.2 MPa) for ZPP are recommended to produce strong, durable bonds between resin cement and zirconia ceramics.

Original languageEnglish (US)
Article numbere101174
JournalPloS one
Issue number7
StatePublished - Jul 3 2014

ASJC Scopus subject areas

  • General


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