Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models

M. Bail; J. Malacarne-Zanon; S. M.A. Silva; A. Anauate-Netto; F. D. Nascimento; R. Amore; H. Lewgoy; D. H. Pashley; M. R. Carrilho

doi:10.1007/s10856-011-4541-y

Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models

M. Bail, J. Malacarne-Zanon, S. M.A. Silva, A. Anauate-Netto, F. D. Nascimento, R. Amore, H. Lewgoy, D. H. Pashley, M. R. Carrilho

Oral Biology

Research output: Contribution to journal › Article › peer-review

21 Scopus citations

Abstract

This study evaluated protocols to eliminate acetone from dental adhesives and their effect on the kinetic of water sorption and percent of conversion of these adhesives. Experimental methacrylate-based adhesives with increasing hydrophilicity (R2, R3, R5) were used as reference materials. Primer-like solutions were prepared by addition of 50 wt% acetone. Acetone elimination was measured gravimetrically before and after: a spontaneous evaporation, an application of air-drying at room temperature or application of 40°C air-drying. Protocols were performed from 15 to 60 s. Specimens of adhesive/ acetone mixtures were photo-activated and tested for degree of conversion, water sorption and solubility. Data were analyzed by ANOVA and Bonferroni's tests (a = 0.05). Complete acetone elimination was never achieved, but it was significantly greater after the 40°C airdrying application. Higher acetone elimination was observed for the least hydrophilic adhesive. Longer periods for acetone evaporation and heated air-stream can optimize polymerization and reduce the water sorption/solubility of adhesive system models.

Original language	English (US)
Pages (from-to)	629-638
Number of pages	10
Journal	Journal of Materials Science: Materials in Medicine
Volume	23
Issue number	3
DOIs	https://doi.org/10.1007/s10856-011-4541-y
State	Published - Mar 2012

ASJC Scopus subject areas

Biophysics
Bioengineering
Biomaterials
Biomedical Engineering

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Bail, M., Malacarne-Zanon, J., Silva, S. M. A., Anauate-Netto, A., Nascimento, F. D., Amore, R., Lewgoy, H., Pashley, D. H., & Carrilho, M. R. (2012). Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models. Journal of Materials Science: Materials in Medicine, 23(3), 629-638. https://doi.org/10.1007/s10856-011-4541-y

Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models. / Bail, M.; Malacarne-Zanon, J.; Silva, S. M.A.; Anauate-Netto, A.; Nascimento, F. D.; Amore, R.; Lewgoy, H.; Pashley, D. H.; Carrilho, M. R.

In: Journal of Materials Science: Materials in Medicine, Vol. 23, No. 3, 03.2012, p. 629-638.

Research output: Contribution to journal › Article › peer-review

Bail, M, Malacarne-Zanon, J, Silva, SMA, Anauate-Netto, A, Nascimento, FD, Amore, R, Lewgoy, H, Pashley, DH & Carrilho, MR 2012, 'Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models', Journal of Materials Science: Materials in Medicine, vol. 23, no. 3, pp. 629-638. https://doi.org/10.1007/s10856-011-4541-y

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title = "Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models",

abstract = "This study evaluated protocols to eliminate acetone from dental adhesives and their effect on the kinetic of water sorption and percent of conversion of these adhesives. Experimental methacrylate-based adhesives with increasing hydrophilicity (R2, R3, R5) were used as reference materials. Primer-like solutions were prepared by addition of 50 wt% acetone. Acetone elimination was measured gravimetrically before and after: a spontaneous evaporation, an application of air-drying at room temperature or application of 40°C air-drying. Protocols were performed from 15 to 60 s. Specimens of adhesive/ acetone mixtures were photo-activated and tested for degree of conversion, water sorption and solubility. Data were analyzed by ANOVA and Bonferroni's tests (a = 0.05). Complete acetone elimination was never achieved, but it was significantly greater after the 40°C airdrying application. Higher acetone elimination was observed for the least hydrophilic adhesive. Longer periods for acetone evaporation and heated air-stream can optimize polymerization and reduce the water sorption/solubility of adhesive system models.",

author = "M. Bail and J. Malacarne-Zanon and Silva, {S. M.A.} and A. Anauate-Netto and Nascimento, {F. D.} and R. Amore and H. Lewgoy and Pashley, {D. H.} and Carrilho, {M. R.}",

note = "Funding Information: Acknowledgments This study was performed by Michele Bail as partial fulfillment of her M.S. degree at the University of Campinas. The authors gratefully acknowledge the technical support given by Mr. Marcos Blanco Cangiani and the editorial assistance of Ms. Michelle Barnes. The experimental resins used in this study were developed and donated by Bisco, Inc. This study was supported in part by Grants from CAPES, Brazil (P.I. Michele Bail); CNPq #306100/2010-0, FAPESP 07/54618-4 (P.I. Marcela Carrilho) and NIDCR # R01-DE-015306 (P.I. David Pashley).",

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AU - Bail, M.

AU - Malacarne-Zanon, J.

AU - Silva, S. M.A.

AU - Anauate-Netto, A.

AU - Nascimento, F. D.

AU - Amore, R.

AU - Lewgoy, H.

AU - Pashley, D. H.

AU - Carrilho, M. R.

N1 - Funding Information: Acknowledgments This study was performed by Michele Bail as partial fulfillment of her M.S. degree at the University of Campinas. The authors gratefully acknowledge the technical support given by Mr. Marcos Blanco Cangiani and the editorial assistance of Ms. Michelle Barnes. The experimental resins used in this study were developed and donated by Bisco, Inc. This study was supported in part by Grants from CAPES, Brazil (P.I. Michele Bail); CNPq #306100/2010-0, FAPESP 07/54618-4 (P.I. Marcela Carrilho) and NIDCR # R01-DE-015306 (P.I. David Pashley).

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N2 - This study evaluated protocols to eliminate acetone from dental adhesives and their effect on the kinetic of water sorption and percent of conversion of these adhesives. Experimental methacrylate-based adhesives with increasing hydrophilicity (R2, R3, R5) were used as reference materials. Primer-like solutions were prepared by addition of 50 wt% acetone. Acetone elimination was measured gravimetrically before and after: a spontaneous evaporation, an application of air-drying at room temperature or application of 40°C air-drying. Protocols were performed from 15 to 60 s. Specimens of adhesive/ acetone mixtures were photo-activated and tested for degree of conversion, water sorption and solubility. Data were analyzed by ANOVA and Bonferroni's tests (a = 0.05). Complete acetone elimination was never achieved, but it was significantly greater after the 40°C airdrying application. Higher acetone elimination was observed for the least hydrophilic adhesive. Longer periods for acetone evaporation and heated air-stream can optimize polymerization and reduce the water sorption/solubility of adhesive system models.

AB - This study evaluated protocols to eliminate acetone from dental adhesives and their effect on the kinetic of water sorption and percent of conversion of these adhesives. Experimental methacrylate-based adhesives with increasing hydrophilicity (R2, R3, R5) were used as reference materials. Primer-like solutions were prepared by addition of 50 wt% acetone. Acetone elimination was measured gravimetrically before and after: a spontaneous evaporation, an application of air-drying at room temperature or application of 40°C air-drying. Protocols were performed from 15 to 60 s. Specimens of adhesive/ acetone mixtures were photo-activated and tested for degree of conversion, water sorption and solubility. Data were analyzed by ANOVA and Bonferroni's tests (a = 0.05). Complete acetone elimination was never achieved, but it was significantly greater after the 40°C airdrying application. Higher acetone elimination was observed for the least hydrophilic adhesive. Longer periods for acetone evaporation and heated air-stream can optimize polymerization and reduce the water sorption/solubility of adhesive system models.

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Effect of air-drying on the solvent evaporation, degree of conversion and water sorption/solubility of dental adhesive models

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